Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source
Category
Published on
Type
journal-article
Author
Y. Feng and R. Alonso-Mori and T. R. M. Barends and V. D. Blank and S. Botha and M. Chollet and D. S. Damiani and R. B. Doak and J. M. Glownia and J. M. Koglin and H. T. Lemke and M. Messerschmidt and K. Nass and S. Nelson and I. Schlichting and R. L. Shoeman and Yu. V. Shvyd'ko and M. Sikorski and S. Song and S. Stoupin and S. Terentyev and G. J. Williams and D. Zhu and A. Robert and S. Boutet
Citation
Feng, Y. et al., 2015. Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source. J Synchrotron Rad, 22(3), pp.626–633. Available at: http://dx.doi.org/10.1107/s1600577515003999.
Abstract
Multiplexing of the Linac Coherent Light Source beam was demonstrated for hard X-rays by spectral division using a near-perfect diamond thin-crystal monochromator operating in the Bragg geometry. The wavefront and coherence properties of both the reflected and transmitted beams were well preserved, thus allowing simultaneous measurements at two separate instruments. In this report, the structure determination of a prototypical protein was performed using serial femtosecond crystallography simultaneously with a femtosecond time-resolved XANES studies of photoexcited spin transition dynamics in an iron spin-crossover system. The results of both experiments using the multiplexed beams are similar to those obtained separately, using a dedicated beam, with no significant differences in quality.